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In order to develop a selective, reliable, sensitive and rapid capillary electrophoretic method for the simultaneous determination of 17 polycyclic aromatic hydrocarbons (PAHs) in environmental samples, the method conditions of separation and electrochemical detection were optimized. The effects of separation voltage, buffer pH, separation buffer concentration and background electrolytes were investigated to optimize the separation and the separation buffer was composed of 50 mmol/L Na-phosphate and 30 mmol/L boric acid. A separation buffer with pH 6.8 was used as the optimum separation buffer. The PAHs were separated within 8 min. Under the optimized conditions, linear ranges of calibration curves (c(PAHs) = 0.1-100 μg/L) were obtained with correlation coefficients (r(2)) of >0.9996. The limits of detection (LOD) were in the range of 0.8-11.5 ng/mL for the 17 PAHs. The relative standard deviations (RSDs, n = 10) were between 0.08-1.8% for the 17 PAHs. The recovery ranged from 97.2-103.4% and reproducibility (RSD) ranged from 1.3-6.5%. The results show that this method can be used for the determination of PAHs in various environmental matrices.Use of a Split Calvarium Flap During Hindfoot Reconstruction to Reduce Complications.
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from setuptools import setup, find_packages
description=”Monastic Run Manager Batch Processor.”,
keywords=[‘monastic’, ‘run’,’master’, ‘worker’],
license=’Apache License 2.0′,
long_description=’Monastic-batch is a user interface for Monastic cluster. It is developed by alibaba team.’,
‘Intended Audience :: Developers’,
‘License :: OSI Approved ::